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KITALYSIS-24PD Sigma-Aldrich

KitAlysis High-Throughput 24 Pd Precatalyst Reaction Screening Kit-Pack of 2

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Description

Application

Screening kit for cross-coupling reactions. Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks.
Step-by-Step Guide for KitAlysis High-Throughput Palladium Precatalyst Cross-Coupling Reaction Screening Kit

Each kit contains 2 customizable screening sets that include the following components:
• 24 pre-weighed catalysts in glass micro vials loaded with stir bars and topped with cap mat.
• 2 KitAlysis 24-Well reaction block replacement films.
• 4 empty substrate stock solution reaction vials with stir bars.
• 3 stir bars for stock solutions.
• 1 internal standard.

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

Features and Benefits

• Designed and tested by synthetic chemists.
• Easily run 24-microscale reaction in parallel.
• Suggested conditions: 10 μmol reactions with 1 μmol catalyst (10 mol%) 0.1 M concentration, and 3 equiv. base.
• Customizable and downloadable excel template for quick calculations and easy incorporation into electronic laboratory notebooks.

Legal Information

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

Safety & Documentation

Safety Information

RIDADR 
UN 3082 9 / PGIII
Protocols & Articles

Articles

KitAlysis High-Throughput Palladium Precatalyst Cross-Coupling Reaction Screening Kit

The screening sets come pre-loaded with 1 µmol of catalyst in each vial according to the following design.  
Keywords: Coupling reactions, Cross couplings, High performance liquid chromatography

KitAlysis™ 24-Well Reaction Block and Screwdriver Set

KitAlysis™ 24-Well Reaction Block KitAlysis™ Torque Screwdriver set KitAlysis™ Reaction Block Replacement Screws (10)
Keywords: Coupling reactions, Cross couplings

KitAlysis™ Benchtop Inertion Box

The Aldrich® KitAlysis™ Benchtop Inertion Box provides an inert environment to run oxygen sensitive cross-coupling reactions easily and robustly in a laboratory fume hood.
Keywords: Coupling reactions, Cross couplings

KitAlysis™ High-Throughput Screening Platform

In the high-pressure environment of discovery chemistry, time is everything. While general catalytic methods exist, substrate dependency makes it difficult to predict optimal conditions in practice. ...
Keywords: Catalysis, Chemical reactions, Solvents

Scale-Up Guide: Palladium Precatalyst Cross-Coupling Reaction Screening Kit

All of the catalysts used in the kit are sensitive to air and moisture in their commercially available form. Please see the catalyst MSDS or product detail page for details on handling and storage. T...
Keywords: Coupling reactions, Cross couplings, PAGE, Solvents

Protocols

Protocol -KitAlysis High-Throughput Palladium Precatalyst Cross-Coupling Reaction Screening Kit

24 pre-weighed Palladium Precatalysts Useful for:  Suzuki-Miyaura Buchwald-Hartwig Negishi Heck  Sonagashira Borylation Ni/Pd co catalyst screen
Keywords: Addition reactions, High performance liquid chromatography, PAGE, Solvents, Thin layer chromatography

Related Content

Catalysis for Screening: KitAlysis™ [VIDEO]

Take a quick look at our latest technology. Now any chemist can quickly and efficiently screen 24 unique cross-coupling reaction conditions with an off-the-shelf kit designed by leading global pharma...
Keywords: Coupling reactions, Cross couplings, PAGE

KitAlysis™ High-Throughput Screening Kits: A Visual Introductory Guide [VIDEO]

This KitAlysis™ High-Throughput Screening Kits video animation clearly illustrates the step by step process that enables any chemist to quickly and efficiently screen 24 unique cross-coupling reactio...
Keywords: Coupling reactions, Cross couplings

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