• USA Home
  • KITALYSIS-BOR - KitAlysis High-Throughput Miyaura Borylation Reaction Screening Kit-Pack of 2

EMAIL THIS PAGE TO A FRIEND
KITALYSIS-BOR Sigma-Aldrich

KitAlysis High-Throughput Miyaura Borylation Reaction Screening Kit-Pack of 2

Purchase

Description

Application

Screening kit for Miyaura borylation reaction. Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks.
Step-by-Step Guide for Miyaura Borylation Reaction Screening Kit
Downloadable Experiment excel sheets

Each kit contains 2 customizable screening sets that include the following components:
• 6 x 4 pre-weighed catalysts in glass vials loaded with stir bars and topped with cap mat.
• 4 x 4 mL reaction vials with pre-weighed KOAc
• Bis(pinacolato)diboron (473294), tetrahydroxydiboron (754242), and pinacol (221171)
• 1 (2 mL) ampule each of toluene, THF, n-butanol, DMA, MeOH, MeCN, ethylene glycol and DIPEA.
• 1 NEW KitAlysis 24-Well Reaction Block Replacement Film.
• 4 stir bars for substrate stock solution vials.
• 1 internal standard.

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

Features and Benefits

• Designed and tested by synthetic chemists.
• Easily run 24-microscale reactions in parallel.
• 10 μmol reactions with 1 μmol catalyst, 3 equiv. base, 0.1 M concentration.
• Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks.

Legal Information

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

Kit component also available separately

Description

Product #

Add to Cart

P(Cy3) Pd G3, 97% SDS 764175
Potassium acetate, anhydrous, free-flowing, Redi-Dri, ACS reagent, ≥99.0% SDS 791733
XPhos Pd G4, 95% SDS 804274
SPhos Pd G4 SDS 804282
RuPhos Pd G4 SDS 804290
DTBPF-Pd-G3 SDS 804975
cataCXium Pd G4 SDS 900349
Toluene, anhydrous, ZerO2®, 99.8% SDS 900522
Ethylene glycol, anhydrous, ZerO2®, 99.8% SDS 900631
N,N-Dimethylacetamide, anhydrous, ZerO2®, 99.8% SDS 900634
Tetrahydrofuran, anhydrous, inhibitor-free, ZerO2®, ≥99.9% SDS 900636
1-Butanol, anhydrous, ZerO2®, 99.8% SDS 900639
Methanol, anhydrous, ZerO2®, 99.8% SDS 900641
Acetonitrile, anhydrous, ZerO2®, 99.8% SDS 900644
Pinacol, 98% SDS 221171
Bis(pinacolato)diboron, 99% SDS 473294
Tetrahydroxydiboron, 95% SDS 754242
Biphenyl, ReagentPlus®, 99.5% SDS B34656
Spinbar® magnetic stirring fleas, red, L × diam. 10 mm × 3 mm SDS Z118850
KitAlysis 24-well reaction block replacement film SDS Z742110
Safety & Documentation

Safety Information

RIDADR 
UN 3316 9
Protocols & Articles

Articles

KitAlysis™ 24-Well Reaction Block and Screwdriver Set

KitAlysis™ 24-Well Reaction Block KitAlysis™ Torque Screwdriver set KitAlysis™ Reaction Block Replacement Screws (10)
Keywords: Coupling reactions, Cross couplings

KitAlysis™ Benchtop Inertion Box

The Aldrich® KitAlysis™ Benchtop Inertion Box provides an inert environment to run oxygen sensitive cross-coupling reactions easily and robustly in a laboratory fume hood.
Keywords: Coupling reactions, Cross couplings

KitAlysis™ High-Throughput Screening Platform

In the high-pressure environment of discovery chemistry, time is everything. While general catalytic methods exist, substrate dependency makes it difficult to predict optimal conditions in practice. ...
Keywords: Catalysis, Chemical reactions, Solvents

Protocols

Protocol KitAlysis™ High-Throughput Miyaura Borylation Reaction Screening Kit

2 bases (KOAc, DIEA) 6 degassed solvents (toluene, DMA, THF, n-butanol, MeOH, MeCN) 6 pre-weighed catalysts (x4)
Keywords: Addition reactions, Derivatizations, High performance liquid chromatography, Miyaura Borylation Reaction, PAGE, Solvents, Thin layer chromatography

Related Content

Catalysis for Screening: KitAlysis™ [VIDEO]

Take a quick look at our latest technology. Now any chemist can quickly and efficiently screen 24 unique cross-coupling reaction conditions with an off-the-shelf kit designed by leading global pharma...
Keywords: Coupling reactions, Cross couplings, PAGE

Related Products

related product

Product #

Description

Add to Cart

Z742064 KitAlysis Benchtop Inertion Box
Z742107 KitAlysis 24-well Reaction Block and Screwdriver Set
Z742108 KitAlysis 24-well Reaction Block and Inertion Box Combination Starter Set
KITALYSIS-CN KitAlysis High-Throughput Buchwald-Hartwig Amination Reaction Screening Kit-Pack of 4
KITALYSIS-SM KitAlysis High-Throughput Suzuki-Miyaura Cross-Coupling Reaction Screening Kit - Pack of 4
KITALYSIS-RCM KitAlysis High-Throughput Medium (5, 6, 7) Ring Closing Metathesis Reaction Screening Kit - Pack of 2
KITALYSIS-24PD KitAlysis High-Throughput 24 Pd Precatalyst Reaction Screening Kit-Pack of 2
900211 Buchwald Precatalyst C-N Coupling Validation Kit
KITALYSIS-CUCN KitAlysis High-Throughput Copper C-N Cross-Coupling Reaction Screening Kit-Pack of 2
KITALYSISBASE KitAlysis High-Throughput Base Screening Kit - Pack of 2

Technical Service:

Our team of scientists has experience in all areas of research including Life Science, Material Science, Chemical Synthesis, Chromatography, Analytical and many others.

Bulk Ordering & Pricing:

Need larger quantities for your development, manufacturing or research applications?