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Z742064 Sigma-Aldrich

KitAlysis Benchtop Inertion Box

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Description

General description

Provides an inert environment to run oxygen sensitive cross-coupling reactions in a laboratory fume hood.
Designed to be used with KitAlysis High-Throughput Screening Kits and KitAlysis 24-Well Reaction Block.

Features and Benefits

• Run 24 micro-scale reactions in parallel under an inert atmosphere.
• Provides a constant flow of inert gas over working area.
• Easy attachment of tubing (not included) from inert gas valve on hood or stand-alone tank.

Legal Information

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

Safety & Documentation

Safety Information

Safety Information for this product is unavailable at this time.

Documents

Certificate of Analysis

Protocols & Articles

Articles

KitAlysis High-Throughput Copper C-N Cross-Coupling Reaction Screening Kit

The screening sets come pre-loaded with 4 µmol of ligand in each vial according to the following design.  
Keywords: Cross couplings, High performance liquid chromatography, Ligands

KitAlysis High-Throughput Metal Scavenger Reaction Screening Kit

The screening sets come pre-loaded with 12 scavengers / resins (10mg or 50mg) in each vial according to the following design.
Keywords: Metal scavengers

KitAlysis High-Throughput Palladium Precatalyst Cross-Coupling Reaction Screening Kit

The screening sets come pre-loaded with 1 µmol of catalyst in each vial according to the following design.  
Keywords: Coupling reactions, Cross couplings, High performance liquid chromatography

KitAlysis Suzuki-Miyaura Cross-Coupling Screening Kit

The screening sets come pre-loaded with 1 µmol of catalyst in each vial according to the following design.
Keywords: Cross couplings, High performance liquid chromatography, Ligands

KitAlysis™ 24-Well Reaction Block and Screwdriver Set

KitAlysis™ 24-Well Reaction Block KitAlysis™ Torque Screwdriver set KitAlysis™ Reaction Block Replacement Screws (10)
Keywords: Coupling reactions, Cross couplings

KitAlysis™ Benchtop Inertion Box

The Aldrich® KitAlysis™ Benchtop Inertion Box provides an inert environment to run oxygen sensitive cross-coupling reactions easily and robustly in a laboratory fume hood.
Keywords: Coupling reactions, Cross couplings

KitAlysis™ C-N (Buchwald-Hartwig) High-Throughput Screening Kit

The screening sets come pre-loaded with 1 µmol of catalyst in each vial according to the following design.
Keywords: Cross couplings, High performance liquid chromatography, Ligands, Solvents

KitAlysis™ High-Throughput Base Reaction Screening Kit

The screening sets come pre-loaded with 30 µmol of base in each vial according to the following design.
Keywords: Coupling reactions, Cross couplings, High performance liquid chromatography, Ligands, Solvents

KitAlysis™ High-Throughput Miyaura Borylation Reaction Screening Kit

The screening sets come pre-loaded with 30 µmol of base in each vial according to the following design.
Keywords: Coupling reactions, Cross couplings, High performance liquid chromatography, Solvents

KitAlysis™ High-Throughput Photocatalysis Reaction Screening Kit

The screening sets come pre-loaded with 30 µmol of base in each vial according to the following design.
Keywords: Coupling reactions, Cross couplings, High performance liquid chromatography, Infrared spectroscopy, Solvents

KitAlysis™ High-Throughput Screening Platform

In the high-pressure environment of discovery chemistry, time is everything. While general catalytic methods exist, substrate dependency makes it difficult to predict optimal conditions in practice. ...
Keywords: Catalysis, Chemical reactions, Solvents

Photo KitAlysis™ Photoreactor Controller

1. Plug in the LED array to the rear panel of the controller marked LED Output. Turn the milliamp intensity knob fully clockwise before powering up the controller.

Ring Closing Metathesis Reaction Screening Kit Materials

The screening sets come pre-loaded with 1 µmol of catalyst in each vial according to the following design.
Keywords: High performance liquid chromatography, Metathesis, Ring-closing metathesis

Protocols

Medium (5,6,7) Ring-Closing Metathesis Procedure

4 degassed solvents: Chlorobenzene (ClPh), Toluene (PhMe), Isopropyl Acetate (i-PrOAc), and Methyl-THF (Me-THF)
Keywords: Addition reactions, Cross metathesis, High performance liquid chromatography, Isomerizations, Metathesis, Olefin metathesis, Solvents, Thin layer chromatography

One Solvent (DMAc), two bases (NaOtBu, Cs2CO3) Step-by-Step Guide for Buchwald-Hartwig Amination Reaction Screening Kit

Solutions & slurries to make: Go to the online user set-up page to enter molecular weights into the downloadable excel file.
Keywords: Addition reactions, Aminations, Buchwald-Hartwig amination, High performance liquid chromatography, PAGE, Thin layer chromatography

One Solvent (Dioxane), two bases (NaOtBu, Cs2CO3) Step-by-Step Guide for Buchwald-Hartwig Amination Reaction Screening Kit

Solutions & slurries to make: Go to the online user set-up page to enter molecular weights into the downloadable excel file.
Keywords: Addition reactions, Aminations, Buchwald-Hartwig amination, High performance liquid chromatography, PAGE, Thin layer chromatography

Protocol KitAlysis™ High-Throughput Base Reaction Screening Kit

7 pre-weighed bases 4 base solutions (DBU (neat), Et3N (neat), LiHMDS (1.0 M in THF), and NaOtBu (2.0 M in THF)) 4 solvents (MeOH, Toluene, DMF, and THF)
Keywords: Addition reactions, High performance liquid chromatography, Ligands, PAGE, Solvents, Thin layer chromatography

Protocol KitAlysis™ High-Throughput Miyaura Borylation Reaction Screening Kit

2 bases (KOAc, DIEA) 6 degassed solvents (toluene, DMA, THF, n-butanol, MeOH, MeCN) 6 pre-weighed catalysts (x4)
Keywords: Addition reactions, Derivatizations, High performance liquid chromatography, Miyaura Borylation Reaction, PAGE, Solvents, Thin layer chromatography

Step-by-Step Guide for KitAlysis™ High-Throughput Photocatalysis Reaction Screening Kit

Note: While the above scheme depicts a generic decarboxylative coupling reaction, High-Throughput Photocatalysis Screening Kit can be used for any photocatalytic transformation
Keywords: Addition reactions, Coupling reactions, High performance liquid chromatography, PAGE, Solvents, Thin layer chromatography, transformation

Suzuki-Miyaura Cross-Coupling Screening Kit Protocol

1 base (K3PO4, 1.5 M solution in degassed water) 4 degassed solvents (DMAc, Toluene, n-Butanol, and THF) 6 pre-weighed catalysts (x4)
Keywords: Addition reactions, Coupling reactions, Cross couplings, High performance liquid chromatography, PAGE, Solvents, Thin layer chromatography

Two solvents (Dioxane, DMAc), strong base (NaOt-Bu) Step-by-Step Guide for Buchwald-Hartwig Amination Reaction Screening Kit

Solutions & slurries to make: Go to the online user set-up page to enter molecular weights into the downloadable excel file.
Keywords: Addition reactions, Aminations, Buchwald-Hartwig amination, High performance liquid chromatography, PAGE, Solvents, Thin layer chromatography

Two solvents (Dioxane, DMAc), weak base (Cs2CO3) Step-by-Step Guide for Buchwald-Hartwig Amination Screening Kit

1 base (Cs2CO3, ground and sieved) 2 solvents (1,4 Dioxane and DMAc) 12 pre-weighed catalysts
Keywords: Addition reactions, Aminations, Buchwald-Hartwig amination, High performance liquid chromatography, PAGE, Solvents, Thin layer chromatography

Related Content

KitAlysis™ High-Throughput Screening Kits: A Visual Introductory Guide [VIDEO]

This KitAlysis™ High-Throughput Screening Kits video animation clearly illustrates the step by step process that enables any chemist to quickly and efficiently screen 24 unique cross-coupling reactio...
Keywords: Coupling reactions, Cross couplings

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