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Z742108 Sigma-Aldrich

KitAlysis 24-well Reaction Block and Inertion Box Combination Starter Set

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Description

General description

The perfect KitAlysis Labware starter kit that combines the KitAlysis Inertion Box (Z742064) with the KitAlysis 24-Well Reaction Block and Screwdriver Set (Z742107).

Provides an inert environment to run oxygen sensitive cross-coupling reactions in a laboratory fume hood.
Designed to be used with KitAlysis High-Throughput Screening Kits.

Components:
• Ιnertion Box
• 24-Well Reaction Block
• Torque Screwdriver set with bit
• Reaction Block Replacement Screws (10ea)

Features and Benefits

Inertion Box
• Run 24 micro-scale reactions in parallel under an inert atmosphere.
• Provides a constant flow of inert gas over working area.
• Easy attachment of tubing (not included) from inert gas valve on hood or stand-alone tank

24-well Reaction Block and Screwdriver Set
• Torque Screwdriver specially designed to seal the block for minimal solvent loss while heating at elevated temperatures.
• Torque setting prevents over-tightening and stripping of screws.
• Includes small screwdriver to easily remove torqued screws after reaction is complete.

Legal Information

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

Safety & Documentation

Safety Information

Safety Information for this product is unavailable at this time.
Protocols & Articles

Articles

KitAlysis High-Throughput Copper C-N Cross-Coupling Reaction Screening Kit

The screening sets come pre-loaded with 4 µmol of ligand in each vial according to the following design.  
Keywords: Cross couplings, High performance liquid chromatography, Ligands

KitAlysis High-Throughput Metal Scavenger Reaction Screening Kit

The screening sets come pre-loaded with 12 scavengers / resins (10mg or 50mg) in each vial according to the following design.
Keywords: Metal scavengers

KitAlysis High-Throughput Palladium Precatalyst Cross-Coupling Reaction Screening Kit

The screening sets come pre-loaded with 1 µmol of catalyst in each vial according to the following design.  
Keywords: Coupling reactions, Cross couplings, High performance liquid chromatography

KitAlysis Suzuki-Miyaura Cross-Coupling Screening Kit

The screening sets come pre-loaded with 1 µmol of catalyst in each vial according to the following design.
Keywords: Cross couplings, High performance liquid chromatography, Ligands

KitAlysis™ 24-Well Reaction Block and Screwdriver Set

KitAlysis™ 24-Well Reaction Block KitAlysis™ Torque Screwdriver set KitAlysis™ Reaction Block Replacement Screws (10)
Keywords: Coupling reactions, Cross couplings

KitAlysis™ Benchtop Inertion Box

The Aldrich® KitAlysis™ Benchtop Inertion Box provides an inert environment to run oxygen sensitive cross-coupling reactions easily and robustly in a laboratory fume hood.
Keywords: Coupling reactions, Cross couplings

KitAlysis™ C-N (Buchwald-Hartwig) High-Throughput Screening Kit

The screening sets come pre-loaded with 1 µmol of catalyst in each vial according to the following design.
Keywords: Cross couplings, High performance liquid chromatography, Ligands, Solvents

KitAlysis™ High-Throughput Base Reaction Screening Kit

The screening sets come pre-loaded with 30 µmol of base in each vial according to the following design.
Keywords: Coupling reactions, Cross couplings, High performance liquid chromatography, Ligands, Solvents

KitAlysis™ High-Throughput Miyaura Borylation Reaction Screening Kit

The screening sets come pre-loaded with 30 µmol of base in each vial according to the following design.
Keywords: Coupling reactions, Cross couplings, High performance liquid chromatography, Solvents

KitAlysis™ High-Throughput Photocatalysis Reaction Screening Kit

The screening sets come pre-loaded with 30 µmol of base in each vial according to the following design.
Keywords: Coupling reactions, Cross couplings, High performance liquid chromatography, Infrared spectroscopy, Solvents

KitAlysis™ High-Throughput Screening Platform

In the high-pressure environment of discovery chemistry, time is everything. While general catalytic methods exist, substrate dependency makes it difficult to predict optimal conditions in practice. ...
Keywords: Catalysis, Chemical reactions, Solvents

Ring Closing Metathesis Reaction Screening Kit Materials

The screening sets come pre-loaded with 1 µmol of catalyst in each vial according to the following design.
Keywords: High performance liquid chromatography, Metathesis, Ring-closing metathesis

Protocols

Medium (5,6,7) Ring-Closing Metathesis Procedure

4 degassed solvents: Chlorobenzene (ClPh), Toluene (PhMe), Isopropyl Acetate (i-PrOAc), and Methyl-THF (Me-THF)
Keywords: Addition reactions, Cross metathesis, High performance liquid chromatography, Isomerizations, Metathesis, Olefin metathesis, Solvents, Thin layer chromatography

One Solvent (DMAc), two bases (NaOtBu, Cs2CO3) Step-by-Step Guide for Buchwald-Hartwig Amination Reaction Screening Kit

Solutions & slurries to make: Go to the online user set-up page to enter molecular weights into the downloadable excel file.
Keywords: Addition reactions, Aminations, Buchwald-Hartwig amination, High performance liquid chromatography, PAGE, Thin layer chromatography

One Solvent (Dioxane), two bases (NaOtBu, Cs2CO3) Step-by-Step Guide for Buchwald-Hartwig Amination Reaction Screening Kit

Solutions & slurries to make: Go to the online user set-up page to enter molecular weights into the downloadable excel file.
Keywords: Addition reactions, Aminations, Buchwald-Hartwig amination, High performance liquid chromatography, PAGE, Thin layer chromatography

Protocol KitAlysis™ High-Throughput Base Reaction Screening Kit

7 pre-weighed bases 4 base solutions (DBU (neat), Et3N (neat), LiHMDS (1.0 M in THF), and NaOtBu (2.0 M in THF)) 4 solvents (MeOH, Toluene, DMF, and THF)
Keywords: Addition reactions, High performance liquid chromatography, Ligands, PAGE, Solvents, Thin layer chromatography

Protocol KitAlysis™ High-Throughput Miyaura Borylation Reaction Screening Kit

2 bases (KOAc, DIEA) 6 degassed solvents (toluene, DMA, THF, n-butanol, MeOH, MeCN) 6 pre-weighed catalysts (x4)
Keywords: Addition reactions, Derivatizations, High performance liquid chromatography, Miyaura Borylation Reaction, PAGE, Solvents, Thin layer chromatography

Suzuki-Miyaura Cross-Coupling Screening Kit Protocol

1 base (K3PO4, 1.5 M solution in degassed water) 4 degassed solvents (DMAc, Toluene, n-Butanol, and THF) 6 pre-weighed catalysts (x4)
Keywords: Addition reactions, Coupling reactions, Cross couplings, High performance liquid chromatography, PAGE, Solvents, Thin layer chromatography

Two solvents (Dioxane, DMAc), strong base (NaOt-Bu) Step-by-Step Guide for Buchwald-Hartwig Amination Reaction Screening Kit

Solutions & slurries to make: Go to the online user set-up page to enter molecular weights into the downloadable excel file.
Keywords: Addition reactions, Aminations, Buchwald-Hartwig amination, High performance liquid chromatography, PAGE, Solvents, Thin layer chromatography

Two solvents (Dioxane, DMAc), weak base (Cs2CO3) Step-by-Step Guide for Buchwald-Hartwig Amination Screening Kit

1 base (Cs2CO3, ground and sieved) 2 solvents (1,4 Dioxane and DMAc) 12 pre-weighed catalysts
Keywords: Addition reactions, Aminations, Buchwald-Hartwig amination, High performance liquid chromatography, PAGE, Solvents, Thin layer chromatography

Related Content

KitAlysis™ High-Throughput Screening Kits: A Visual Introductory Guide [VIDEO]

This KitAlysis™ High-Throughput Screening Kits video animation clearly illustrates the step by step process that enables any chemist to quickly and efficiently screen 24 unique cross-coupling reactio...
Keywords: Coupling reactions, Cross couplings

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